Cryogen Instruments India Pvt. Ltd.

Institute of Chemical Technology, Mumbai

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Workshop on NMR

High Field NMR FFC NMR Relaxometry
  • Introduction
  • Basics of NMR
  • Structure by 1D & 2D NMR
  • Introduction of FFC (Fast Field Cycling)
  • Applications of FFC Relaxometry
(Agenda & Program Overleaf)

Dates: 17 th – 18 th October 2022

Venue: Institute of Chemical Technology, Mumbai


Registrations :

Registration Fee:

Registration Category Online Live Webinar
ICT Faculty / Students N/A
University/Academeia ₹250
Industry Delegates ₹2500

Seats Availability:

Registration Category Online Live Webinar
ICT Faculty / Students N/A
University/Academeia 50
Industry Delegates 200

For Registration Form: https://meet.zoho.com/XQdjULFI08

Download Brochure:

Registration starts on 1st October 2022 and ends on 15th October 2022

Registrations will be confirmed on 1st come 1st serve basis, as limited seats are available

Payment: 1) DD in Favor of M/S Cryogen Instruments India Pvt Ltd., Payable at Thane.

2) Online Payment: A/C No. 04240200009897, IFSC Code: BARBOTHANAX

For Inquiries & Registration:

ICT Faculty/Students Industry Delegates/University Students
  • Convenor:
  • Dr. G.S.Shankarling
  • Dept. of Speciality Chemicals
  • Institute of Chemical Technology
  • N.P.Marg, Matunga, Mumbai 400 019
  • Email: gs.shankarling@ictmumbai.edu.in

Workshop Programme

Day 1 – Basics of NMR

NMR - Introduction & Basics:Covers basics of NMR spectroscopy mathematical treatment, energy levels, Larmor equation, resonance condition, brief introduction to instrumentation, extractable parameters from NMR spectrum - chemical shift and coupling constants, definition of chemical shift, shielding and deshielding, chemical shift scale, origin of coupling constants, Pascal's triangle, spin-spin splitting, splitting pattern, aliphatic and aromatic molecules as examples to decipher chemical shift and coupling constant, introduction to C13 NMR, interaction between H1-C13, decoupling, practical approach to NMR, sample handling, integration, quantitative NMR, introduction to 2D NMR, Homonuclear and Heteronuclear 2D NMR experiments for structural elucidation, summary

Structure by NMR: Information from 1D and 2D NMR experiments, overview of NMR experiments used for structural elucidation, Observables from homo-nuclear and hetero-nuclear 2D NMR experiments, identification of spin systems, establishing connectivity, mapping homo-nuclear and hetero-nuclear coupling constants, exploiting long-range hetero-nuclear coupling constants, determining fragments and connecting fragments, deriving the skeleton of the molecule, elucidating the structure of a saccharide molecule.

Show & Tell NMR: A walk through on 500 MHz NMR spectrometer, detailed explanation of superconducting magnet, hardware, probe, and software, sample preparation guidelines and checkpoints, workflow of analysis, data processing.

Day 2 – Advance NMR Techniques – 2D, QNMR (Quantification), FFC Relaxometry

Structure by 2D NMR Information from 1D and 2D NMR experiments, overview of NMR experiments used for structural elucidation, Observables from homo-nuclear and hetero-nuclear 2D NMR experiments, identification of spin systems, establishing connectivity, mapping homo-nuclear and hetero-nuclear coupling constants, exploiting long-range hetero-nuclear coupling constants, determining fragments and connecting fragments, deriving the skeleton of the molecule, elucidating the structure of a saccharide molecule.

qNMR(Quantification by NMR): Introduction to qNMR, usage of qNMR, concentration and purity determination, calibration standard, practical aspects, importance of experimental conditions, integration and peak analysis, calculations to determine concentration and purity, a couple of practical examples.

FFC Relaxometer: The power of Fast Field Cycling NMR relaxometry as an analytical technique Introduction to Fast Field Cycling (FFC) as a low-field NMR technique [1] which allows the measurement of the T1 (or R1=1/T1) of a sample over a wide range of magnetic field strengths (from 10kHz to 40MHz) using just one instrument. How FFC finds application in many different sectors such as: MRI contrast agents, liquids in confined spaces (e.g. oil-bearing rocks and catalysts), electrolytes, proteins, batteries, foodstuff and plastic/polymers industry.

Day 1 (Monday)

Introduction to Basic NMR & Demo

Date Sessions Topics Time
17th
October
2022
Inauguration & Opening Speech 01.30 pm to 02.00 pm
Session 1 Introduction & Basics of NMR 02.00 pm to 03.30 pm
Tea / Coffee Break 03.30 pm to 03.45 pm
Session 2 Structure Determination by NMR 03.45 pm to 05.15 pm
Session 3 Interaction, Q&A 05.15 pm to 05.30 pm

Day 2 (Tuesday)

Advance NMR Techniques & FFC Relaxometry(For Industry)

Date Sessions Topics Time
18th
October
2022
Session 4 Structure By 2D NMR 09.30 am to 11.00 am
Tea / Coffee Break 11.00 am to 11.30 am
Session 5 Advance NMR Techniques (2D/QNMR) 11.30 am to 01.00 pm
Lunch Break 01.00 pm to 02.00 pm
Session 6 FFC NMR Relaxometry Introduction 02.00 pm to 03.00 pm
Tea / Coffee Break 03.00 pm to 3.30 pm
Session 7 FFC relaxometry Applications 03.30 pm to 04.30 pm
session 8 Interaction, Q&A 04.30 pm to 05.00 pm